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ICP-OES MICS Đọc trực tiếp quang phổ đầy đủ quang phổ quang phổ phát thải plasma kết nối cảm ứng

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Detector

Máy dò rắn CCD làm mát bán dẫn hiệu quả với pixel liên tục trong phạm vi bước sóng của quang phổ, cho phép lựa chọn bước sóng tùy ý và được thiết kế với chức năng chống tràn ngập tự nhiên

(1) Dđơn vị etectingHơn 3000000 đơn vị phát hiện, tốc độ đọc≥2MHz

(2) Độ phân giải pixel≤0.003nm

(3) Detector refrigeration systemTo achieve the lowest detector dark current, efficient three-stage semiconductor cooling is used

(4) Refrigeration temperature-45℃Time to reach working temperature< 3 minute

(5) Optical systemConstant temperature driven stepped spectroscopic system

(6) MonochromatorMid step grating and prism two-dimensional dispersion systemHigh energy,to ensure the stability of instrument testing, internal optical components such as gratings and prisms are fixed in position, and all elements are measured simultaneously in one exposure across the full wavelength range of the spectrometer

(7) X-ray roomxEquipped with precision light chamber constant temperature 35℃-40℃Argon or nitrogen can be used for purging the light chamberWhen measuring the<200nm spectral line, the gas       displacement is<3L/min

(8) Wavelength coverage165-900nmFull wavelength coverage

(9) Optical resolutionFHW):As189.042nm half width<0.007nmCa393.366nm half width<0.017nmBa614.172 half width<0.024nm, K766.490nm half width<0.035nm,To ensure the stability and optimal luminous flux of the optical system

Plasma

(1) Plasma observation methodVertical placement of torch tube

(2) RF generatorSolid-state generatorThe plasma coil is designed with a PTFE protective layer, which  is corrosion-resistant and maintenance free

(3) Frequency27.12MHZ

(4) RF power500-1600W

(5) Pneumatic controlConfigure 3 high-precision quality flow controllers, directly controlled by ICP-OES   software, including cooling gas, auxiliary gas, and atomization gasPrecision0.01 L/min

(6) Peristaltic pump5-channel 16-roller peristaltic pump

Performance analysis 

(1) Analysis speed≥50 elements or spectral lines per minuteAnd the integration time of each measured spectral line≥10s

(2) Sample consumption<2mlDetermine more than 70 elements

(3) Spectral line flexibilityQualitative, semi-quantitative and quantitative analysis can be conducted on any spectral line of the analyzed element, which is convenient for analysis and research

(4) Measure the linear dynamic range of spectral lines≥106Measured with Mn257.6nm, correlation     coefficient ≥0.9996),Provide supporting documents

(5) Internal standard calibrationSimultaneous internal standard calibration, which means that both internal standard elements and measurement elements must be exposed simultaneously

(6) PrecisionDetermination of 1ppm or 10ppm multi-element mixed standard solutionRSD ≤ 0.5% for   repeated measurements of ten times

StabilityDetermination of 1ppm or 10ppm multi-element mixed standard solutiondo not use internal standard calibrationContinuous 4-hour long-term stability RSD<1.0%

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